Welcome to Nanalysis’ benchtop NMR Blog
We love benchtop NMR! In this blog section, you will find all things benchtop NMR. Please contact us if you would like to discuss about your project.
Category
NMR Topics
- 100 MHz NMR
- 11B NMR
- 129Xe NMR
- 13C NMR
- 19F NMR
- 19F NMR Spectroscopy
- 1H NMR
- 207Pb NMR
- 31P NMR
- 3H NMR
- 60 MHz NMR
- APT
- Agrochemicals
- Applications
- Batteries
- Biochemistry
- Biopolymers
- Botanicals
- COSY
- CPMG
- Caffeine Content
- Cannabis
- Chemical Analysis
- Cosmetics
- DEPT
- Dithiazine
- Drug Analysis
- Drug Discovery
- Dyes
- Edible Oils
- Educational NMR
- Energy
- Enzyme
- Exchangeable Protons
- Exchangeable protons
- Flavor and Fragrances
- Flow NMR
- Fluorine-19 NMR
- Food Science
- Food and Beverage
- Forensics
- Forestry
- HETCOR
- HMBC
- HSQC
- Hands-on Learning
- Heteronuclear J-coupling
- Hydrogen sulfide
- Hydroxyl value
- Hyphenated NMR
Spicing Up Your Holidays with NMR
If there is one thing that I could say describes the holiday season best, it would have to be the delicious treats I get to indulge in, such as: gingerbread cookies, pies, peppermint bark, and so many more. Wafting in the aroma of baked goods always gives me butterflies in my stomach and lights up my nuclear magnetic resonance (NMR) mind.
Unsymmetric Carbon Satellites in Fluorine-19 NMR
In the 19F NMR spectrum of DCBTF, we can observe the singlet resonance of the trifluoromethyl fragment at δ = −63.07 ppm. While it might not jump into your eye at first glance, please note that the carbon satellites are not centered at the "main signal", which is what we are used to from 1H NMR spectra. Read more
Eat Your Heart Out Mass Spec: Measuring 10B/11B Isotopic Ratio by NMR Spectroscopy
As I’m sure the readers of this blog know, NMR spectroscopy is used widely across all branches of chemistry due to its powerful structure elucidation capabilities and the inherently quantitative nature of the technique. Organic relies primarily on 1H/13C experiments where as inorganic chemistry can expand to other nuclei, like 31P and 11B. However, there are many other applications for NMR other than just structural elucidation. Perhaps a lesser known application of NMR spectroscopy, is its ability to determine the isotopic ratio of elements! In this blog post I would like to demonstrate a novel method to determine the 10B/11B isotopic ratio using our NMReady-60e and 1H NMR spectra!
Eat Your Heart Out Mass Spec: Measuring 10B/11B Isotopic Ratio by NMR Spectroscopy
As I’m sure the readers of this blog know, NMR spectroscopy is used widely across all branches of chemistry due to its powerful structure elucidation capabilities and the inherently quantitative nature of the technique. Organic relies primarily on 1H/13C experiments where as inorganic chemistry can expand to other nuclei, like 31P and 11B. However, there are many other applications for NMR other than just structural elucidation. Perhaps a lesser known application of NMR spectroscopy, is its ability to determine the isotopic ratio of elements! In this blog post I would like to demonstrate a novel method to determine the 10B/11B isotopic ratio using our NMReady-60e and 1H NMR spectra!
Candy Corn or Candy Corn-not
Let’s talk about Candy Corn and ask the question: what is really in candy? One thing I have noticed is that the nutritional facts on the back of the candy bag can be somewhat misleading.
Two solvents, two different spectra - Aromatic Solvent Induced Shifts
In my opinion, one of the most helpful papers[1] in the field of NMR spectroscopy in Organic Chemistry consists of ‘just’ two tables. In these, the chemical shifts (1H and 13C) of as many as forty-two common impurities in twelve different deuterated solvents are listed. This is gold! Why?
Quantifying Battery Additives with the 60PRO
In this ever-evolving world where technology and science keep pushing into new territory, new inventions are being made and state-of-the-art validation methods are being developed. Over the last few decades, lithium-ion batteries have gained more and more traction in their uses, moving from general simple batteries used for powering your calculator or phone, to cars and trucks, and even airplanes (currently only the small ones). However, as simple as batteries may seem, a lot of work must be done behind to scenes to develop these subtle but priceless additions to our lives.
Process-NMR – Future key elements in the world of Process Analytical Technology (PAT)
What is process analytical technology (PAT) and why is it so important?PAT is an extremely powerful and useful tool for analyzing, optimizing and controlling chemical processes. Chemical, food and pharmaceutical industries could especially benefit from this technique. In earlier days, chemical processes were primarily monitored by physical techniques, such as temperature, pH, pressure etc..
Tritium NMR?! What’s that look like?
Hello fellow NMR enthusiasts, have you ever wondered what tritium (3H) looks like via NMR? I know I have, and today, I would like to share some data with you. Read noww.
NOESY: the experiment for when you just need to know more, particularly the 1H-1H spatial proximity
Given the superior resolution of our 100 MHz instrument, we can perform structure elucidation on increasingly large molecules. As molecules get more complex, as do the suite of experiments that can be used to…